HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-methyl-3-(methyl-phenyl-carbamoyl)-3H-imidazol-1-ium iodide → Methyl-phenyl-carbamic acid 4-(2-cyclohexyl-acetylamino)-phenyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-methyl-3-(methyl-phenyl-carbamoyl)-3H-imidazol-1-ium iodide | HCID 10947884 | — |
| Reactant | 2-Cyclohexyl-N-(4-hydroxy-phenyl)-acetamide | HCID 22047780 | — |
| Product | Methyl-phenyl-carbamic acid 4-(2-cyclohexyl-acetylamino)-phenyl ester | HCID 10287026 | 77.5% |
Reaction Steps
The title compound (284 mg, 77% yield, white crystals) was prepared from 2-cyclohexyl-N-(4-hydroxy-phenyl)-acetamide (233 mg, 1.00 mmol) and 1-methyl-3-(methyl-phenyl—carbamoyl)-3H-imidazol-1-ium iodide (343 mg, 1.00 mmol). HPLC-MS m/z=367 (M+1); Rt=4.51 min
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07279470B2 |
| Source dataset | uspto-grants-2007_10 |
| ORD ID | ord-76364c926bca4a7b8bbe367d4bff41ea |
| Source note | uspto-grants-2007_10 |