HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-methyl-3-(methyl-phenyl-carbamoyl)-3H-imidazol-1-ium iodide → Methyl-phenyl-carbamic Acid 4-(3,3-dimethyl-butyrylamino)-phenyl Ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-methyl-3-(methyl-phenyl-carbamoyl)-3H-imidazol-1-ium iodide | HCID 10947884 | — |
| Reactant | N-(4-Hydroxyphenyl)-3,3-dimethylbutanamide | HCID 22047740 | — |
| Product | Methyl-phenyl-carbamic Acid 4-(3,3-dimethyl-butyrylamino)-phenyl Ester | HCID 10172155 | 77% |
Reaction Steps
The title compound (262 mg, 77% yield) was prepared from N-(4-hydroxyphenyl)-3,3-dimethyl-butyramide (275 mg, 1.00 mmol) and 1-methyl-3-(methyl-phenyl-carbamoyl)-3H-imidazol-1-ium iodide (343 mg, 1.00 mmol). HPLC-MS m/z=341 (M+1); Rt=4.15 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07279470B2 |
| Source dataset | uspto-grants-2007_10 |
| ORD ID | ord-793b4c0c8f0f4173928e59e7f1b5972e |
| Source note | uspto-grants-2007_10 |