3-Benzyl-4-methylumbelliferone → HCID 10309678, compound

HRID 1179734Notes

Reaction equation

HRID 1179734 reaction equation
[CH2:1]([C:8]1[C:9](=[O:20])[O:10][C:11]2[C:16]([C:17]=1[CH3:18])=[CH:15][CH:14]=[C:13]([OH:19])[CH:12]=2)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[I-].[CH3:22][N:23]([C:32]1[CH:37]=[CH:36][CH:35]=[CH:34][CH:33]=1)[C:24](N1C=C[N+](C)=C1)=[O:25]>>[CH2:1]([C:8]1[C:9](=[O:20])[O:10][C:11]2[C:16]([C:17]=1[CH3:18])=[CH:15][CH:14]=[C:13]([O:19][C:24](=[O:25])[N:23]([CH3:22])[C:32]1[CH:37]=[CH:36][CH:35]=[CH:34][CH:33]=1)[CH:12]=2)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

Participants

3

Reactant 2

HCID 53385383-Benzyl-4-methylumbelliferoneHCID 109478841-methyl-3-(methyl-phenyl-carbamoyl)-3H-imidazol-1-ium iodide

Product 1

HCID 10309678HCID 10309678, compound

Procedure

The title compound was prepared from 3-benzyl-7-hydroxy-4-methyl-2H-chromen-2-one and 3-(methyl-phenyl-carbamoyl)-1-methyl-3H-imidazol-1-ium iodide. HPLC-MS m/z=400 (M+1), Rt: 4.90 min.

Sources & evidence

ORD record
ord-6bf1fe2b1296421eb96a8abb01164448
Source dataset
uspto-grants-2007_10
Patent number
US07279470B2

Reaction notes

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