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HRID1179743

反应详情

EQUATION

反应方程式

HRID 1179743 的结构方程式

REACTANTS

反应物

2
结构：Oc1ccc(Oc2ccc(C(F)(F)F)cn2)cc1
HCID155241

4-[[5-(Trifluoromethyl)-2-pyridinyl]oxy]phenol

C12H8F3NO2

结构：CN(C(=O)n1cc[n+](C)c1)c1ccc(Cl)cc1.[I-]
HCID22047798

未命名化合物

PRODUCTS

生成物

1
结构：CN(C(=O)Oc1ccc(Oc2ccc(C(F)(F)F)cn2)cc1)c1ccc(Cl)cc1
HCID10310052

4-[[5-(Trifluoromethyl)-2-pyridinyl]oxy]phenyl N-(4-chlorophenyl)-N-methylcarbamate

C20H14ClF3N2O3

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCCCCCC.CCOC(C)=O
溶剂HCID21899848

未命名化合物

PROCEDURE

实验过程

The title compound was prepared from 4-(5-trifluoromethyl-pyridin-2-yloxy)-phenol and 3[(4-chlorophenyl)-methyl-carbamoyl]-1-methyl-3H-imidazol-1-ium iodide. The crude product was subjected to flash chromatography (ethyl acetate/heptan, 1:5) (77%, white crystals). HPLC-MS m/z=423.1 (M+1), Rt: 5.3 min.