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HRID1179746

反应详情

EQUATION

反应方程式

HRID 1179746 的结构方程式

REACTANTS

反应物

2
结构：CCN(C(=O)Cl)c1ccccc1
HCID96376

Ethyl(phenyl)carbamoyl chloride

C9H10ClNO

结构：Oc1ccc(Oc2ccc(C(F)(F)F)cc2)cc1
HCID170230

4-[(4-Trifluoromethylphenyl)oxy]phenol

C13H9F3O2

PRODUCTS

生成物

1
结构：CCN(C(=O)Oc1ccc(Oc2ccc(C(F)(F)F)cc2)cc1)c1ccccc1
HCID10150786

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCCCCCC.CCOC(C)=O
溶剂HCID21899848

未命名化合物

PROCEDURE

实验过程

The title compound was prepared from 4-(4-trifluoromethyl-phenoxy)-phenol and N-ethyl-N-phenylcarbamoyl chloride. The crude product was subjected to flash chromatography (ethyl acetate/heptane, 1:5) (77%, white crystals. HPLC-MS m/z=402.1 (M+1), Rt: 5.6 min.