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HRID1179757

反应详情

EQUATION

反应方程式

HRID 1179757 的结构方程式

REACTANTS

反应物

2
结构：Oc1ccc(Oc2ccc(C(F)(F)F)cn2)cc1
HCID155241

4-[[5-(Trifluoromethyl)-2-pyridinyl]oxy]phenol

C12H8F3NO2

结构：CC1CCCN(C(=O)n2cc[n+](C)c2)C1.[I-]
HCID43145417

未命名化合物

PRODUCTS

生成物

1
结构：CC1CCCN(C(=O)Oc2ccc(Oc3ccc(C(F)(F)F)cn3)cc2)C1
HCID23635634

未命名化合物

PROCEDURE

实验过程

The title compound was prepared from 4-(5-trifluoromethyl-pyridin-2-yloxy)-phenol and 1-methyl-3-(3-methyl-piperidine-1-carbonyl)-3H-imidazol-1-ium iodide. The crude product was purified by flash chromatography using a Quad flash 25 (ethyl acetate/heptane (1:6), (75%, white crystals). HPLC-MS m/z=381.1 (M+1), Rt: 5.4 min.

WORKUP

后处理

  1. customThe crude product was purified by flash chromatography