4-(3,5-Dichloro-pyridin-2-yloxy)-phenol → HCID 69520314, compound

HRID 1179761Notes

Reaction equation

HRID 1179761 reaction equation
[Cl:1][C:2]1[C:3]([O:9][C:10]2[CH:15]=[CH:14][C:13]([OH:16])=[CH:12][CH:11]=2)=[N:4][CH:5]=[C:6]([Cl:8])[CH:7]=1.[I-].[N:18]1([C:28](N2C=C[N+](C)=C2)=[O:29])[C:27]2[C:22](=[CH:23][CH:24]=[CH:25][CH:26]=2)[CH2:21][CH2:20][CH2:19]1>>[Cl:1][C:2]1[C:3]([O:9][C:10]2[CH:15]=[CH:14][C:13]([O:16][C:28]([N:18]3[C:27]4[C:22](=[CH:23][CH:24]=[CH:25][CH:26]=4)[CH2:21][CH2:20][CH2:19]3)=[O:29])=[CH:12][CH:11]=2)=[N:4][CH:5]=[C:6]([Cl:8])[CH:7]=1

Participants

3

Reactant 2

HCID 6208804-(3,5-Dichloro-pyridin-2-yloxy)-phenolHCID 109595761-(3,4-Dihydroquinolin-1(2H)-ylcarbonyl)-3-methyl-1H-imidazol-3-ium Iodide

Product 1

HCID 69520314HCID 69520314, compound

Procedure

The title compound was prepared from 4-(3,5-dichloro-pyridin-2-yloxy)-phenol and 3-(3,4-dihydro-2H-quinoline-1-carbonyl)-1-methyl-3H-imidazol-1-ium iodide. The crude product was recrystallized (ethanol) (68%). HPLC-MS m/z=415.2 (M+1), Rt: 5.6 min.

Workup

  1. customThe crude product was recrystallized (ethanol) (68%)

Sources & evidence

ORD record
ord-72ca60f00ab74d75b111dcdd9f9fec05
Source dataset
uspto-grants-2007_10
Patent number
US07279470B2

Reaction notes

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