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HRID1179776

反应详情

EQUATION

反应方程式

HRID 1179776 的结构方程式

REACTANTS

反应物

2
结构：O=C(Cl)N1CCOCC1
HCID84810

4-Morpholinecarbonyl chloride

C5H8ClNO2

结构：Oc1ccc(Oc2ncc(Cl)cc2Cl)cc1
HCID620880

4-[(3,5-dichloropyridin-2-yl)oxy]phenol

C11H7Cl2NO2

PRODUCTS

生成物

1
结构：O=C(Oc1ccc(Oc2ncc(Cl)cc2Cl)cc1)N1CCOCC1
HCID23635767

未命名化合物

PROCEDURE

实验过程

The title compound was prepared from 4-(3,5-dichloro-pyridin-2-yloxy)-phenol and morpholine-4-carbonyl chloride. The crude product was purified by preparative HPLC (45%, crystals. HPLC-MS m/z=369.1 (M+1), Rt: 4.3 min.

WORKUP

后处理

  1. customThe crude product was purified by preparative HPLC (45%, crystals