huagongshe.com
HRID1179777

反应详情

EQUATION

反应方程式

HRID 1179777 的结构方程式

REACTANTS

反应物

2
结构：O=C(Cl)N1CCOCC1
HCID84810

4-Morpholinecarbonyl chloride

C5H8ClNO2

结构：Cc1c(Cc2ccc(F)cc2)c(=O)oc2cc(O)ccc12
HCID5924338

未命名化合物

PRODUCTS

生成物

1
结构：Cc1c(Cc2ccc(F)cc2)c(=O)oc2cc(OC(=O)N3CCOCC3)ccc12
HCID86589204

未命名化合物

PROCEDURE

实验过程

The title compound was prepared from 3-(4-fluorobenzyl)-7-hydroxy-4-methyl-2H-chromen-2-one and morpholine-4-carbonyl chloride. The crude product was recrystallized (ethanol) (78%, crystals). HPLC-MS m/z=398.0 (M+1), Rt: 4.3 min.

WORKUP

后处理

  1. customThe crude product was recrystallized (ethanol) (78%, crystals)