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HRID1179784

反应详情

EQUATION

反应方程式

HRID 1179784 的结构方程式

REACTANTS

反应物

2
结构：CN(C(=O)Cl)c1ccccc1
HCID77969

Carbamic chloride, methylphenyl-

C8H8ClNO

结构：On1cccn1
HCID3016733

1H-Pyrazol-1-ol

C3H4N2O

PRODUCTS

生成物

1
结构：CN(C(=O)On1cccn1)c1ccccc1
HCID10149109

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCCCCCC.CCOC(C)=O
溶剂HCID21899848

未命名化合物

PROCEDURE

实验过程

The title compound was prepared from 1-hydroxypyrazole and N-methyl-N-phenylcarbamoyl chloride. The crude product was subjected to flash chromatography (Quad flash 25, EtOAc-heptane) (79%, oil which slowly crystallizes). HPLC-MS m/z=218.1 (M+1), Rt: 2.82 min. Mp 63-67° C.

WORKUP

后处理

  1. customslowly crystallizes)