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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1179785Generated: November 3, 2026

Carbamic chloride, N-methyl-N-phenyl- → HCID 10286262, compound

https://huagongshe.com/reaction/1179785

Reaction equation

Participants

RoleNameHCIDCharge
ReactantCarbamic chloride, N-methyl-N-phenyl-HCID 77969—
Reactant1-Hydroxy-4-bromopyrazoleHCID 11744951—
SolventEthylacetate heptaneHCID 21899848—
ProductHCID 10286262HCID 10286262—

Reaction Steps

The title compound was prepared from 1-hydroxy-4-bromopyrazole and N-methyl-N-phenylcarbamoyl chloride. The crude product was subjected to flash chromatography (Quad flash 25, EtOAc-heptane) (89%, oil). HPLC-MS m/z=298.0 (M+1), Rt: 3.77 min.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07279470B2
Source datasetuspto-grants-2007_10
ORD IDord-a6c315395ea44d42a93debbe5f910e3a
Source noteuspto-grants-2007_10