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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1179787Generated: October 31, 2026

Carbamic chloride, N-methyl-N-phenyl- → HCID 10285903, compound

https://huagongshe.com/reaction/1179787

Reaction equation

Participants

RoleNameHCIDCharge
ReactantCarbamic chloride, N-methyl-N-phenyl-HCID 77969—
ReactantHCID 10877052HCID 10877052—
SolventEthylacetate heptaneHCID 21899848—
ProductHCID 10285903HCID 10285903—

Reaction Steps

The title compound was prepared from 1-hydroxy-1,2,3-triazole and N-methyl-N-phenylcarbamoyl chloride. The crude product was subjected to flash chromatography (Quad flash 25, EtOAc-heptane) (80%, oil). HPLC-MS m/z=219.1 (M+1), Rt: 2.50 min. Mp 105-106° C.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07279470B2
Source datasetuspto-grants-2007_10
ORD IDord-4d23c193e8af47f7a8cff406a13e1717
Source noteuspto-grants-2007_10