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HRID1179790

反应详情

EQUATION

反应方程式

HRID 1179790 的结构方程式

REACTANTS

反应物

2
结构：CN(C(=O)Cl)c1ccccc1
HCID77969

Carbamic chloride, methylphenyl-

C8H8ClNO

结构：N#CCCc1ccc(O)cc1
HCID87079

3-(4-Hydroxyphenyl)propanenitrile

C9H9NO

PRODUCTS

生成物

1
结构：CN(C(=O)Oc1ccc(CCC#N)cc1)c1ccccc1
HCID69519626

未命名化合物

PROCEDURE

实验过程

The title product was prepared from 3-(4-hydroxyphenyl)proprionitrile and N-methyl-N-phenylcarbamoyl chloride. The crude product was subjected to preparative HPLC (11%, colourless oil). HPLC-MS: m/z=281.2 (M+1); Rt: 3.75 min, purity 80%.