4'-Hydroxyacetophenone → HCID 2929356, compound

HRID 1179794Notes

Reaction equation

HRID 1179794 reaction equation
[OH:1][C:2]1[CH:7]=[CH:6][C:5]([C:8](=[O:10])[CH3:9])=[CH:4][CH:3]=1.[CH3:11][N:12]([C:16]1[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=1)[C:13](Cl)=[O:14]>>[C:8]([C:5]1[CH:6]=[CH:7][C:2]([O:1][C:13](=[O:14])[N:12]([CH3:11])[C:16]2[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=2)=[CH:3][CH:4]=1)(=[O:10])[CH3:9]

Participants

3

Reactant 2

HCID 74694'-HydroxyacetophenoneHCID 77969Carbamic chloride, N-methyl-N-phenyl-

Product 1

HCID 2929356HCID 2929356, compound

Procedure

The title product was prepared from 4′-hydroxyacetophenone and N-methyl-N-phenylcarbamoyl chloride. The crude product was subjected to preparative HPLC. (78%, colourless oil). HPLC-MS: m/z=270.1 (M+1); Rt: 3.62 min.

Sources & evidence

ORD record
ord-c09d625d773b47948e032eb933bf4a53
Source dataset
uspto-grants-2007_10
Patent number
US07279470B2

Reaction notes

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