Carbamic chloride, N-methyl-N-phenyl- → HCID 10376468, compound

HRID 1179795Notes

Reaction equation

HRID 1179795 reaction equation
[OH:1][C:2]1[CH:7]=[CH:6][N:5]=[CH:4][CH:3]=1.[CH3:8][N:9]([C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1)[C:10](Cl)=[O:11]>>[N:5]1[CH:6]=[CH:7][C:2]([O:1][C:10](=[O:11])[N:9]([CH3:8])[C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=2)=[CH:3][CH:4]=1

Participants

3

Reactant 2

HCID 77969Carbamic chloride, N-methyl-N-phenyl-HCID 178418642HCID 178418642, compound

Product 1

HCID 10376468HCID 10376468, compound

Procedure

The title product was prepared from 4-hydroxypyridine and N-methyl-N-phenylcarbamoyl chloride. The crude product was subjected to preparative HPLC. (11%, yellow solid). HPLC-MS: m/z=229.2 (M+1); Rt: 1.66 min, purity: 67%.

Sources & evidence

ORD record
ord-1fac46dbc1514ed0884ee80c4e4e6b4c
Source dataset
uspto-grants-2007_10
Patent number
US07279470B2

Reaction notes

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