Carbamic chloride, N-methyl-N-phenyl- → HCID 69520782, compound

HRID 1179809Notes

Reaction equation

HRID 1179809 reaction equation
[OH:1][C:2]1[CH:7]=[CH:6][C:5]([C:8](=[O:23])[CH:9]=[CH:10][C:11]2[CH:16]=[C:15]([O:17][CH3:18])[C:14]([O:19][CH3:20])=[C:13]([O:21][CH3:22])[CH:12]=2)=[CH:4][CH:3]=1.[CH3:24][N:25]([C:29]1[CH:34]=[CH:33][CH:32]=[CH:31][CH:30]=1)[C:26](Cl)=[O:27]>>[CH3:22][O:21][C:13]1[CH:12]=[C:11]([CH:10]=[CH:9][C:8]([C:5]2[CH:6]=[CH:7][C:2]([O:1][C:26](=[O:27])[N:25]([CH3:24])[C:29]3[CH:34]=[CH:33][CH:32]=[CH:31][CH:30]=3)=[CH:3][CH:4]=2)=[O:23])[CH:16]=[C:15]([O:17][CH3:18])[C:14]=1[O:19][CH3:20]

Participants

3

Reactant 2

HCID 77969Carbamic chloride, N-methyl-N-phenyl-HCID 2600711-(4-hydroxyphenyl)-3-(3,4,5-trimethoxyphenyl)prop-2-en-1-one

Product 1

HCID 69520782HCID 69520782, compound

Procedure

The title product was prepared from 1-(4-hydroxyphenyl)-3-(3,4,5-trimethoxyphenyl)prop-2-en-1-one and N-methyl-N-phenylcarbamoyl chloride. The crude product was subjected to preparative HPLC (82%, yellow solid). HPLC-MS: m/z=448.2 (M+1); Rt: 4.61 min.

Sources & evidence

ORD record
ord-fbbef1f3e9ba45ed82ebe3fde7bdd400
Source dataset
uspto-grants-2007_10
Patent number
US07279470B2

Reaction notes

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