HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethamivan → Methyl-phenyl-carbamic Acid 4-diethylcarbamoyl-2-methoxy-phenyl Ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethamivan | HCID 9363 | — |
| Reactant | Carbamic chloride, N-methyl-N-phenyl- | HCID 77969 | — |
| Product | Methyl-phenyl-carbamic Acid 4-diethylcarbamoyl-2-methoxy-phenyl Ester | HCID 69519834 | — |
Reaction Steps
The title product was prepared from N,N-diethyl-4-hydroxy-3-methoxy-benzamide and N-methyl-N-phenylcarbamoyl chloride. The crude product was subjected to preparative HPLC (58%, colorless oil). HPLC-MS: m/z=357.1 (M+1); Rt: 3.64 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07279470B2 |
| Source dataset | uspto-grants-2007_10 |
| ORD ID | ord-b926100beef34922845287d820e3c1cd |
| Source note | uspto-grants-2007_10 |