Carbamic chloride, N-methyl-N-phenyl- → HCID 69518641, compound

HRID 1179811Notes

Reaction equation

HRID 1179811 reaction equation
[OH:1][C:2]1[CH:3]=[C:4]([CH:14]=[CH:15][CH:16]=1)[C:5]([NH:7][C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1)=[O:6].[CH3:17][N:18]([C:22]1[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=1)[C:19](Cl)=[O:20]>>[C:8]1([NH:7][C:5]([C:4]2[CH:3]=[C:2]([O:1][C:19](=[O:20])[N:18]([CH3:17])[C:22]3[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=3)[CH:16]=[CH:15][CH:14]=2)=[O:6])[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1

Participants

3

Reactant 2

HCID 77969Carbamic chloride, N-methyl-N-phenyl-HCID 3389917HCID 3389917, compound

Product 1

HCID 69518641HCID 69518641, compound

Procedure

The title product was prepared from 3-hydroxy-N-phenyl-benzamide and N-methyl-N-phenylcarbamoyl chloride. The crude product was subjected to preparative HPLC (54%, white solid). HPLC-MS: m/z=347.2 (M+1); Rt: 4.01 min.

Sources & evidence

ORD record
ord-6baa1567583c49449eb50e5dfe92e6e4
Source dataset
uspto-grants-2007_10
Patent number
US07279470B2

Reaction notes

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