Carbamic chloride, N-methyl-N-phenyl- → HCID 69518210, compound

HRID 1179812Notes

Reaction equation

HRID 1179812 reaction equation
[OH:1][C:2]1[CH:11]=[C:10]2[C:5]([CH:6]=[CH:7][CH:8]=[N:9]2)=[CH:4][CH:3]=1.[CH3:12][N:13]([C:17]1[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1)[C:14](Cl)=[O:15]>>[N:9]1[C:10]2[C:5](=[CH:4][CH:3]=[C:2]([O:1][C:14](=[O:15])[N:13]([CH3:12])[C:17]3[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=3)[CH:11]=2)[CH:6]=[CH:7][CH:8]=1

Participants

3

Reactant 2

HCID 77969Carbamic chloride, N-methyl-N-phenyl-HCID 1354268667-Hydroxyquinoline

Product 1

HCID 69518210HCID 69518210, compound

Procedure

The title product was prepared from 7-hydroxyquinoline and N-methyl-N-phenylcarbamoyl chloride. The crude product was subjected to preparative HPLC (28%, white solid). HPLC-MS: m/z=279.1 (M+1); Rt: 2.55 min.

Sources & evidence

ORD record
ord-39aa43463fa64d8f95bb310a9c7498fc
Source dataset
uspto-grants-2007_10
Patent number
US07279470B2

Reaction notes

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