3-Hydroxyacetanilide → HCID 69518100, compound

HRID 1179814Notes

Reaction equation

HRID 1179814 reaction equation
[C:1]([NH:4][C:5]1[CH:6]=[C:7]([OH:11])[CH:8]=[CH:9][CH:10]=1)(=[O:3])[CH3:2].[CH3:12][N:13]([C:17]1[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1)[C:14](Cl)=[O:15]>>[C:1]([NH:4][C:5]1[CH:6]=[C:7]([O:11][C:14](=[O:15])[N:13]([CH3:12])[C:17]2[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=2)[CH:8]=[CH:9][CH:10]=1)(=[O:3])[CH3:2]

Participants

3

Reactant 2

HCID 121243-HydroxyacetanilideHCID 77969Carbamic chloride, N-methyl-N-phenyl-

Product 1

HCID 69518100HCID 69518100, compound

Procedure

The title product was prepared from 3-acetamidophenol and N-methyl-N-phenylcarbamoyl chloride. The crude product was subjected to preparative HPLC (66%, white solid). HPLC-MS: m/z=285.1 (M+1); Rt: 3.09 min.

Sources & evidence

ORD record
ord-1c3f8a2f6eb34e8eae9417b4828798a5
Source dataset
uspto-grants-2007_10
Patent number
US07279470B2

Reaction notes

Loading…