4-Hydroxybenzophenone → HCID 2930306, compound

HRID 1179815Notes

Reaction equation

HRID 1179815 reaction equation
[OH:1][C:2]1[CH:7]=[CH:6][C:5]([C:8]([C:10]2[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=2)=[O:9])=[CH:4][CH:3]=1.[CH3:16][N:17]([C:21]1[CH:26]=[CH:25][CH:24]=[CH:23][CH:22]=1)[C:18](Cl)=[O:19]>>[C:8]([C:5]1[CH:4]=[CH:3][C:2]([O:1][C:18](=[O:19])[N:17]([CH3:16])[C:21]2[CH:26]=[CH:25][CH:24]=[CH:23][CH:22]=2)=[CH:7][CH:6]=1)(=[O:9])[C:10]1[CH:11]=[CH:12][CH:13]=[CH:14][CH:15]=1

Participants

3

Reactant 2

HCID 143474-HydroxybenzophenoneHCID 77969Carbamic chloride, N-methyl-N-phenyl-

Product 1

HCID 2930306HCID 2930306, compound

Procedure

The title product was prepared from (4-hydroxy-phenyl)-phenyl-methanone and N-methyl-N-phenylcarbamoyl chloride. The crude product was subjected to preparative HPLC (36%, colorless oil). HPLC-MS: m/z=332.2 (M+1); Rt: 4.42 min.

Sources & evidence

ORD record
ord-4996e1462a6c4bfc98d57d68efa5f360
Source dataset
uspto-grants-2007_10
Patent number
US07279470B2

Reaction notes

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