3-Phenylphenol → HCID 69519069, compound

HRID 1179816Notes

Reaction equation

HRID 1179816 reaction equation
[C:1]1([C:7]2[CH:8]=[C:9]([OH:13])[CH:10]=[CH:11][CH:12]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[CH3:14][N:15]([C:19]1[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=1)[C:16](Cl)=[O:17]>>[C:7]1([C:1]2[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=2)[CH:12]=[CH:11][CH:10]=[C:9]([O:13][C:16](=[O:17])[N:15]([CH3:14])[C:19]2[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=2)[CH:8]=1

Participants

3

Reactant 2

HCID 113813-PhenylphenolHCID 77969Carbamic chloride, N-methyl-N-phenyl-

Product 1

HCID 69519069HCID 69519069, compound

Procedure

The title product was prepared from 3-phenylphenol and N-methyl-N-phenylcarbamoyl chloride. The crude product was subjected to preparative HPLC (52%, colorless oil). HPLC-MS: m/z=304.2 (M+1); Rt: 4.75 min.

Sources & evidence

ORD record
ord-cd746f207f57451c9b23e05bc27ac9af
Source dataset
uspto-grants-2007_10
Patent number
US07279470B2

Reaction notes

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