HuagongsheHuagongshe Chemistry Print Report · For research reference only
4'-Hydroxybutyranilide → Methyl-phenyl-carbamic Acid 4-butyrylamino-phenyl Ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4'-Hydroxybutyranilide | HCID 66874 | — |
| Reactant | Carbamic chloride, N-methyl-N-phenyl- | HCID 77969 | — |
| Product | Methyl-phenyl-carbamic Acid 4-butyrylamino-phenyl Ester | HCID 69519645 | — |
Reaction Steps
The title product was prepared from 4′-hydroxybutyranilide and N-methyl-N-phenylcarbamoyl chloride. The crude product was subjected to preparative HPLC (60%, white solid). HPLC-MS: m/z=313.2 (M+1); Rt: 3.58 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07279470B2 |
| Source dataset | uspto-grants-2007_10 |
| ORD ID | ord-df532a5ea6d146e7a08d6bb5c852fb0c |
| Source note | uspto-grants-2007_10 |