Carbamic chloride, N-methyl-N-phenyl- → HCID 69518361, compound

HRID 1179829Notes

Reaction equation

HRID 1179829 reaction equation
[CH3:1][C:2]1[CH:7]=[C:6]([CH3:8])[N:5]=[C:4]([S:9][C:10]2[CH:15]=[CH:14][C:13]([OH:16])=[CH:12][CH:11]=2)[N:3]=1.[CH3:17][N:18]([C:22]1[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=1)[C:19](Cl)=[O:20]>>[CH3:1][C:2]1[CH:7]=[C:6]([CH3:8])[N:5]=[C:4]([S:9][C:10]2[CH:15]=[CH:14][C:13]([O:16][C:19](=[O:20])[N:18]([CH3:17])[C:22]3[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=3)=[CH:12][CH:11]=2)[N:3]=1

Participants

3

Reactant 2

HCID 77969Carbamic chloride, N-methyl-N-phenyl-HCID 27363074-[(4,6-Dimethylpyrimidin-2-yl)sulfanyl]phenol

Product 1

HCID 69518361HCID 69518361, compound

Procedure

The title product was prepared from 4-(4,6-dimethylpyrimidin-2-ylsulfanyl)-phenol and N-methyl-N-phenylcarbamoyl chloride. The crude product was subjected to preparative HPLC (59%, white solid). HPLC-MS: m/z=366.1 (M+1); Rt: 4.50 min.

Sources & evidence

ORD record
ord-fca90839d6ce4d8195a2225061f780fe
Source dataset
uspto-grants-2007_10
Patent number
US07279470B2

Reaction notes

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