Carbamic chloride, N-methyl-N-phenyl- → HCID 69518877, compound

HRID 1179830Notes

Reaction equation

HRID 1179830 reaction equation
[CH3:1][S:2]([C:5]1[CH:10]=[CH:9][C:8]([OH:11])=[CH:7][CH:6]=1)(=[O:4])=[O:3].[CH3:12][N:13]([C:17]1[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1)[C:14](Cl)=[O:15]>>[CH3:1][S:2]([C:5]1[CH:10]=[CH:9][C:8]([O:11][C:14](=[O:15])[N:13]([CH3:12])[C:17]2[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=2)=[CH:7][CH:6]=1)(=[O:3])=[O:4]

Participants

3

Reactant 2

HCID 77969Carbamic chloride, N-methyl-N-phenyl-HCID 1233504-(Methylsulfonyl)phenol

Product 1

HCID 69518877HCID 69518877, compound

Procedure

The title product was prepared from 4-methylsulfonylphenol and N-methyl-N-phenylcarbamoyl chloride. The crude product was subjected to preparative HPLC (50%, white solid). HPLC-MS: m/z=306.1 (M+1); Rt: 3.22 min.

Sources & evidence

ORD record
ord-9714a353aa964816bfea7d39b2d31bda
Source dataset
uspto-grants-2007_10
Patent number
US07279470B2

Reaction notes

Loading…