Carbamic chloride, N-methyl-N-phenyl- → HCID 69517971, compound

HRID 1179831Notes

Reaction equation

HRID 1179831 reaction equation
[OH:1][C:2]1[CH:7]=[CH:6][C:5]([NH:8][C:9](=[O:22])[CH2:10][CH:11]2[C:20](=[O:21])[NH:19][C:18]3[C:13](=[CH:14][CH:15]=[CH:16][CH:17]=3)[NH:12]2)=[CH:4][CH:3]=1.[CH3:23][N:24]([C:28]1[CH:33]=[CH:32][CH:31]=[CH:30][CH:29]=1)[C:25](Cl)=[O:26]>>[O:21]=[C:20]1[NH:19][C:18]2[C:13](=[CH:14][CH:15]=[CH:16][CH:17]=2)[NH:12][CH:11]1[CH2:10][C:9]([NH:8][C:5]1[CH:6]=[CH:7][C:2]([O:1][C:25](=[O:26])[N:24]([CH3:23])[C:28]2[CH:33]=[CH:32][CH:31]=[CH:30][CH:29]=2)=[CH:3][CH:4]=1)=[O:22]

Participants

3

Reactant 2

HCID 77969Carbamic chloride, N-methyl-N-phenyl-HCID 2879854HCID 2879854, compound

Product 1

HCID 69517971HCID 69517971, compound

Procedure

The title product was prepared from N-(4-hydroxyphenyl)-2-(3-oxo-1,2,3,4-tetrahydro-2-quinoxalinyl)acetamide and N-methyl-N-phenylcarbamoyl chloride. The crude product was subjected to preparative HPLC (20%, yellow solid). HPLC-MS: m/z=431.2 (M+1); Rt: 3.55 min.

Sources & evidence

ORD record
ord-0909bf9d84044ed8a95123646abaf9db
Source dataset
uspto-grants-2007_10
Patent number
US07279470B2

Reaction notes

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