HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-Methylbenzeneethanamine → Methyl-phenyl-carbamic Acid 4-(methyl-phenethyl-carbamoyl)-phenyl Ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-Methylbenzeneethanamine | HCID 11503 | — |
| Reactant | 4-(Methyl-phenyl-carbamoyloxy)-benzoic Acid 2,5-dioxo-pyrrolidin-1-yl Ester | HCID 86589206 | — |
| Product | Methyl-phenyl-carbamic Acid 4-(methyl-phenethyl-carbamoyl)-phenyl Ester | HCID 69518284 | — |
Reaction Steps
The title product was prepared from 4-(methyl-phenyl-carbamoyloxy)-benzoic acid 2,5-dioxo-pyrrolidin-1-yl ester and methyl-phenethyl-amine. The crude product was subjected to preparative HPLC (29%, oil). HPLC-MS: m/z=389.2 (M+1); Rt: 4.15 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07279470B2 |
| Source dataset | uspto-grants-2007_10 |
| ORD ID | ord-71ced6268aa74075a935d02261c3e7b1 |
| Source note | uspto-grants-2007_10 |