1,2-Ethanediamine, N1-phenyl- → HCID 69518667, compound

HRID 1179841Notes

Reaction equation

HRID 1179841 reaction equation
O=C1CCC(=O)N1O[C:9](=[O:27])[C:10]1[CH:15]=[CH:14][C:13]([O:16][C:17](=[O:26])[N:18]([CH3:25])[C:19]2[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=2)=[CH:12][CH:11]=1.[C:28]1([NH:34][CH2:35][CH2:36][NH2:37])[CH:33]=[CH:32][CH:31]=[CH:30][CH:29]=1>>[C:28]1([NH:34][CH2:35][CH2:36][NH:37][C:9]([C:10]2[CH:11]=[CH:12][C:13]([O:16][C:17](=[O:26])[N:18]([CH3:25])[C:19]3[CH:20]=[CH:21][CH:22]=[CH:23][CH:24]=3)=[CH:14][CH:15]=2)=[O:27])[CH:33]=[CH:32][CH:31]=[CH:30][CH:29]=1

Participants

3

Reactant 2

HCID 742701,2-Ethanediamine, N1-phenyl-HCID 865892064-(Methyl-phenyl-carbamoyloxy)-benzoic Acid 2,5-dioxo-pyrrolidin-1-yl Ester

Product 1

HCID 69518667HCID 69518667, compound

Procedure

The title product was prepared from 4-(methyl-phenyl-carbamoyloxy)-benzoic acid 2,5-dioxo-pyrrolidin-1-yl ester and N-phenylethylenediamine. The crude product was used without further purification (80%, off-white foam). HPLC-MS: m/z=390.2 (M+1); Rt: 3.51 min.

Workup

  1. customThe crude product was used without further purification (80%, off-white foam)

Sources & evidence

ORD record
ord-024c65e8895e49b28c71c08a0cf3e410
Source dataset
uspto-grants-2007_10
Patent number
US07279470B2

Reaction notes

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