3,3-Dimethylbutylamine → Methyl-phenyl-carbamic Acid 4-(3,3-dimethyl-butylcarbamoyl)-phenyl Ester

HRID 1179843Notes

Reaction equation

HRID 1179843 reaction equation
O=C1CCC(=O)N1O[C:9](=[O:27])[C:10]1[CH:15]=[CH:14][C:13]([O:16][C:17](=[O:26])[N:18]([CH3:25])[C:19]2[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=2)=[CH:12][CH:11]=1.[CH3:28][C:29]([CH3:34])([CH3:33])[CH2:30][CH2:31][NH2:32]>>[CH3:28][C:29]([CH3:34])([CH3:33])[CH2:30][CH2:31][NH:32][C:9]([C:10]1[CH:11]=[CH:12][C:13]([O:16][C:17](=[O:26])[N:18]([CH3:25])[C:19]2[CH:20]=[CH:21][CH:22]=[CH:23][CH:24]=2)=[CH:14][CH:15]=1)=[O:27]

Participants

3

Reactant 2

HCID 197093,3-DimethylbutylamineHCID 865892064-(Methyl-phenyl-carbamoyloxy)-benzoic Acid 2,5-dioxo-pyrrolidin-1-yl Ester

Product 1

HCID 69518631Methyl-phenyl-carbamic Acid 4-(3,3-dimethyl-butylcarbamoyl)-phenyl Ester

Procedure

The title product was prepared from 4-(methyl-phenyl-carbamoyloxy)-benzoic acid 2,5-dioxo-pyrrolidin-1-yl ester and 3,3-dimethylbutylamine. The crude product was used without further purification (88%, oil). HPLC-MS: m/z=355.1 (M+1); Rt: 3.10 min.

Workup

  1. customThe crude product was used without further purification (88%, oil)

Sources & evidence

ORD record
ord-a4431eaedefd4793909680b0997509a5
Source dataset
uspto-grants-2007_10
Patent number
US07279470B2

Reaction notes

Loading…