Carbamic chloride, N-methyl-N-phenyl- → HCID 10214889, compound

HRID 1179896Notes

Reaction equation

HRID 1179896 reaction equation
[OH:1][N:2]1[CH:6]=[CH:5][C:4]([Br:7])=[N:3]1.[CH3:8][N:9]([C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1)[C:10](Cl)=[O:11]>>[Br:7][C:4]1[CH:5]=[CH:6][N:2]([O:1][C:10](=[O:11])[N:9]([CH3:8])[C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=2)[N:3]=1

Participants

3

Reactant 2

HCID 77969Carbamic chloride, N-methyl-N-phenyl-HCID 15506938HCID 15506938, compound

Product 1

HCID 10214889HCID 10214889, compound

Procedure

The title compound was prepared from 1-hydroxy-3-bromopyrazole and N-methyl-N-phenylcarbamoyl chloride applying the general procedure 8. The crude product was purified by flash chromatography (Quad flash 12, EtOAc-heptane) (63%, oil).

Workup

  1. customThe crude product was purified by flash chromatography (Quad flash 12, EtOAc-heptane) (63%, oil)

Sources & evidence

ORD record
ord-882692f5798d4ceaa2449026e46351ab
Source dataset
uspto-grants-2007_10
Patent number
US07279470B2

Reaction notes

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