Carbamic chloride, N-methyl-N-phenyl- → HCID 10215373, compound

HRID 1179897Notes

Reaction equation

HRID 1179897 reaction equation
[OH:1][N:2]1[C:6]([I:7])=[CH:5][CH:4]=[N:3]1.[CH3:8][N:9]([C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1)[C:10](Cl)=[O:11]>>[I:7][C:6]1[N:2]([O:1][C:10](=[O:11])[N:9]([CH3:8])[C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=2)[N:3]=[CH:4][CH:5]=1

Participants

3

Reactant 2

HCID 77969Carbamic chloride, N-methyl-N-phenyl-HCID 22047934HCID 22047934, compound

Product 1

HCID 10215373HCID 10215373, compound

Procedure

The title compound was prepared from 1-hydroxy-5-iodopyrazole and N-methyl-N-phenylcarbamoyl chloride applying the general procedure 8. The crude product was purified by flash chromatography (Quad flash 12, EtOAc-heptane) (64%, oil).

Workup

  1. customThe crude product was purified by flash chromatography (Quad flash 12, EtOAc-heptane) (64%, oil)

Sources & evidence

ORD record
ord-193515576f914081aefa244ca85e5b71
Source dataset
uspto-grants-2007_10
Patent number
US07279470B2

Reaction notes

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