Carbamic chloride, N-methyl-N-phenyl- → HCID 69519413, compound

HRID 1179900Notes

Reaction equation

HRID 1179900 reaction equation
[OH:1][N:2]1[C:6]([C:7](=[O:14])[C:8]2[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=2)=[CH:5][CH:4]=[N:3]1.[CH3:15][N:16]([C:20]1[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=1)[C:17](Cl)=[O:18]>>[C:7]([C:6]1[N:2]([O:1][C:17](=[O:18])[N:16]([CH3:15])[C:20]2[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=2)[N:3]=[CH:4][CH:5]=1)(=[O:14])[C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1

Participants

3

Reactant 2

HCID 77969Carbamic chloride, N-methyl-N-phenyl-HCID 22048006HCID 22048006, compound

Product 1

HCID 69519413HCID 69519413, compound

Procedure

The title compound was prepared from 1-hydroxy-5-benzoylpyrazole and N-methyl-N-phenylcarbamoyl chloride applying the general procedure 8. The crude product was purified by flash chromatography (Quad flash 12, EtOAc-heptane) (30%, crystals).

Workup

  1. customThe crude product was purified by flash chromatography (Quad flash 12, EtOAc-heptane) (30%, crystals)

Sources & evidence

ORD record
ord-83784273dcc641eabf61c489cebd7323
Source dataset
uspto-grants-2007_10
Patent number
US07279470B2

Reaction notes

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