Carbamic chloride, N-methyl-N-phenyl- → HCID 69519983, compound

HRID 1179902Notes

Reaction equation

HRID 1179902 reaction equation
[OH:1][N:2]1[C:6]([C:7]2[CH:12]=[CH:11][C:10]([N:13]([CH3:15])[CH3:14])=[CH:9][CH:8]=2)=[CH:5][CH:4]=[N:3]1.[CH3:16][N:17]([C:21]1[CH:26]=[CH:25][CH:24]=[CH:23][CH:22]=1)[C:18](Cl)=[O:19]>>[CH3:14][N:13]([CH3:15])[C:10]1[CH:9]=[CH:8][C:7]([C:6]2[N:2]([O:1][C:18](=[O:19])[N:17]([CH3:16])[C:21]3[CH:26]=[CH:25][CH:24]=[CH:23][CH:22]=3)[N:3]=[CH:4][CH:5]=2)=[CH:12][CH:11]=1

Participants

3

Reactant 2

HCID 77969Carbamic chloride, N-methyl-N-phenyl-HCID 22047864HCID 22047864, compound

Product 1

HCID 69519983HCID 69519983, compound

Procedure

The title compound was prepared from 1-hydroxy-5-(4-dimethylaminophenyl)-pyrazole and N-methyl-N-phenylcarbamoyl chloride applying the general procedure 8. The crude product was purified by flash chromatography (Quad flash 12, EtOAc-heptane) (27%, crystals).

Workup

  1. customThe crude product was purified by flash chromatography (Quad flash 12, EtOAc-heptane) (27%, crystals)

Sources & evidence

ORD record
ord-79476f1a6ae540b7a23df2eda30db07b
Source dataset
uspto-grants-2007_10
Patent number
US07279470B2

Reaction notes

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