Carbamic chloride, N-methyl-N-phenyl- → HCID 69519956, compound

HRID 1179906Notes

Reaction equation

HRID 1179906 reaction equation
Cl.[OH:2][N:3]1[CH:7]=[CH:6][N:5]=[C:4]1[S:8][CH3:9].[CH3:10][N:11]([C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1)[C:12](Cl)=[O:13]>>[CH3:9][S:8][C:4]1[N:3]([O:2][C:12](=[O:13])[N:11]([CH3:10])[C:15]2[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=2)[CH:7]=[CH:6][N:5]=1

Participants

3

Reactant 2

HCID 77969Carbamic chloride, N-methyl-N-phenyl-HCID 69520539HCID 69520539, compound

Product 1

HCID 69519956HCID 69519956, compound

Procedure

The title compound was prepared from 1-hydroxy-2-methylsulfanyl-imidazole hydrochloride and N-methyl-N-phenylcarbamoyl chloride applying the general procedure 8. The crude product was purified by flash chromatography (Quad flash 12, EtOAc-heptane) (97%, oil).

Workup

  1. customThe crude product was purified by flash chromatography (Quad flash 12, EtOAc-heptane) (97%, oil)

Sources & evidence

ORD record
ord-020a3fc07da64d2e890a20ccc319e73d
Source dataset
uspto-grants-2007_10
Patent number
US07279470B2

Reaction notes

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