Carbamic chloride, N-methyl-N-phenyl- → HCID 69520707, compound

HRID 1179910Notes

Reaction equation

HRID 1179910 reaction equation
Cl.[OH:2][N:3]1[CH:7]=[CH:6][N:5]=[C:4]1[C:8]1[CH:13]=[CH:12][C:11]([N+:14]([O-:16])=[O:15])=[CH:10][CH:9]=1.[CH3:17][N:18]([C:22]1[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=1)[C:19](Cl)=[O:20]>>[N+:14]([C:11]1[CH:10]=[CH:9][C:8]([C:4]2[N:3]([O:2][C:19](=[O:20])[N:18]([CH3:17])[C:22]3[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=3)[CH:7]=[CH:6][N:5]=2)=[CH:13][CH:12]=1)([O-:16])=[O:15]

Participants

3

Reactant 2

HCID 77969Carbamic chloride, N-methyl-N-phenyl-HCID 131725813HCID 131725813, compound

Product 1

HCID 69520707HCID 69520707, compound

Procedure

The title compound was prepared from 1-hydroxy-2-(4-nitrophenyl)imidazole, hydrochloride and N-methyl-N-phenylcarbamoyl chloride applying the general procedure 8. The crude product was purified by flash chromatography (Quad flash 12, EtOAc-heptane) (90%, yellow crystals).

Workup

  1. customThe crude product was purified by flash chromatography (Quad flash 12, EtOAc-heptane) (90%, yellow crystals)

Sources & evidence

ORD record
ord-6aebee2bc3714e368acd755c85822f95
Source dataset
uspto-grants-2007_10
Patent number
US07279470B2

Reaction notes

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