Carbamic chloride, N-methyl-N-phenyl- → HCID 86589209, compound

HRID 1179912Notes

Reaction equation

HRID 1179912 reaction equation
[OH:1][N:2]1[CH:6]=[C:5]([CH:7]=[O:8])[CH:4]=[N:3]1.[CH3:9][N:10]([C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1)[C:11](Cl)=[O:12]>>[CH:7]([C:5]1[CH:4]=[N:3][N:2]([O:1][C:11](=[O:12])[N:10]([CH3:9])[C:14]2[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=2)[CH:6]=1)=[O:8]

Participants

3

Reactant 2

HCID 77969Carbamic chloride, N-methyl-N-phenyl-HCID 22047945HCID 22047945, compound

Product 1

HCID 86589209HCID 86589209, compound

Procedure

The title compound was prepared from 1-hydroxy-4-formylpyrazole and N-methyl-N-phenylcarbamoyl chloride applying the general procedure 8. The crude product was purified by flash chromatography (Quad flash 12, EtOAc-heptane) (73%, oil).

Workup

  1. customThe crude product was purified by flash chromatography (Quad flash 12, EtOAc-heptane) (73%, oil)

Sources & evidence

ORD record
ord-4d49a21448fd4e3db1cfab3cf0b9a221
Source dataset
uspto-grants-2007_10
Patent number
US07279470B2

Reaction notes

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