HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Morpholinecarbonyl chloride → Morpholine-4-carboxylic Acid 3-(4-methoxy-phenyl)-pyrazol-1-yl Ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Morpholinecarbonyl chloride | HCID 84810 | — |
| Reactant | 1-Hydroxy-3-(4-methoxyphenyl)pyrazole | HCID 11805519 | — |
| Product | Morpholine-4-carboxylic Acid 3-(4-methoxy-phenyl)-pyrazol-1-yl Ester | HCID 69518318 | — |
Reaction Steps
The title compound was prepared from 1-hydroxy-3-(4-methoxyphenyl)pyrazole and 4-morpholine carbonyl chloride applying the general procedure 8. The crude product was purified by flash chromatography (Quad flash 12, EtOAc-heptane) (62%, crystals).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07279470B2 |
| Source dataset | uspto-grants-2007_10 |
| ORD ID | ord-49061d7ef99d4642994b19b367b958fc |
| Source note | uspto-grants-2007_10 |