Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Potassium Bromide → 4-Cyclopropylmethyl-piperazine-1-carboxylic Acid 4-[2-(4-chloro-phenyl)-ethylcarbamoyl]-phenyl Ester
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Potassium Bromide | HCID 253877 | — |
| 반응물 | 1-(Cyclopropylmethyl)piperazine | HCID 965875 | — |
| 반응물 | L-Ascorbic Acid | HCID 54670067 | — |
| 반응물 | 4-[2-(4-Chloro-phenyl)-ethylcarbamoyl]-phenyl chloroformate | HCID 86589213 | — |
| 생성물 | 4-Cyclopropylmethyl-piperazine-1-carboxylic Acid 4-[2-(4-chloro-phenyl)-ethylcarbamoyl]-phenyl Ester | HCID 69520541 | 18% |
반응 단계
The title compound was prepared from 4-[2-(4-chloro-phenyl)-ethylcarbamoyl]-phenyl chloroformate and 1-cyclopropylmethyl-piperazine, yield 18%. White crystals, m.p. 225-226° C.; IR (KBr): ν 1710 (ester C═O), 1661 (amide C═O) cm−1.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07279470B2 |
| 출처 데이터셋 | uspto-grants-2007_10 |
| ORD ID | ord-39541d4c6c2541569022a1c494e6b615 |
| 출처 메모 | uspto-grants-2007_10 |