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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1179964Generated: October 31, 2026

1-Dansylpiperazine → HCID 69519488, compound

https://huagongshe.com/reaction/1179964

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1-DansylpiperazineHCID 11738697—
Reactant4-(5-Trifluoromethylpyridin-2-yloxy)-phenyl chloroformateHCID 22047762—
ProductHCID 69519488HCID 6951948832%

Reaction Steps

The title compound was prepared from 4-(5-trifluoromethyl-pyridin-2-yloxy)-phenyl chloroformate and 1-(5-dimethylamino-naphthalene-1-sulfonyl)-piperazine and purified by flash chromatography (ethyl acetate—heptane 1:4), yield 32%. Pale crystals, HPLC-MS: m/z: 601(M+1) at Rt=5.2 min.; m.p. ° C.; IR (KBr): ν 1723 (C═O) cm−1.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07279470B2
Source datasetuspto-grants-2007_10
ORD IDord-cf0a014e9b6e48319a9aa31ff934f036
Source noteuspto-grants-2007_10