HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(Cyclopropylmethyl)piperazine → 4-Cyclopropylmethyl-piperazine-1-Carboxylic acid 4-(4,4-dimethyl-2,6-dioxo-piperidin-1-yl)-phenyl Ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(Cyclopropylmethyl)piperazine | HCID 965875 | — |
| Reactant | 4-(4,4-Dimethyl-2,6-dioxo-piperidin-1-yl)-phenyl chloroformate | HCID 22047895 | — |
| Product | 4-Cyclopropylmethyl-piperazine-1-Carboxylic acid 4-(4,4-dimethyl-2,6-dioxo-piperidin-1-yl)-phenyl Ester | HCID 57455846 | — |
Reaction Steps
The title compound was prepared from 4-(4,4-dimethyl-2,6-dioxo-piperidin-1-yl)-phenyl chloroformate and 1-cyclopropylmethyl-piperazine, preparative HPLC (Method C) (45%, off-white crystals). HPLC-MS m/z=400.3 (M+1), Rt: 1.83 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07279470B2 |
| Source dataset | uspto-grants-2007_10 |
| ORD ID | ord-cf755149c18c413988c5b00294a7f926 |
| Source note | uspto-grants-2007_10 |