HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-((4-Methoxyphenyl)methyl)piperazine → 4-(4-Methoxy-benzyl)-piperazine-1-carboxylic acid 4-(2-cyclohexyl-acetylamino)-phenyl Ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-((4-Methoxyphenyl)methyl)piperazine | HCID 231905 | — |
| Reactant | 4-(2-Cyclohexyl-acetylamino)-phenyl chloroformate | HCID 22047886 | — |
| Product | 4-(4-Methoxy-benzyl)-piperazine-1-carboxylic acid 4-(2-cyclohexyl-acetylamino)-phenyl Ester | HCID 57473679 | — |
Reaction Steps
The title compound was prepared from 4-(2-cyclohexyl-acetylamino)-phenyl chloroformate and 1-(4-methoxybenzyl)-piperazine, preparative HPLC (Method C) (49%, white crystals). HPLC-MS m/z=466.3 (M+1), Rt: 2.85 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07279470B2 |
| Source dataset | uspto-grants-2007_10 |
| ORD ID | ord-72d30463a4304ebd9dfb8234478ca27f |
| Source note | uspto-grants-2007_10 |