HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(Cyclopropylmethyl)piperazine → 4-Cyclopropylmethyl-piperazine-1-carboxylic acid 4-(2-cyclohexyl-acetylamino)-phenyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(Cyclopropylmethyl)piperazine | HCID 965875 | — |
| Reactant | 4-(2-Cyclohexyl-acetylamino)-phenyl chloroformate | HCID 22047886 | — |
| Product | 4-Cyclopropylmethyl-piperazine-1-carboxylic acid 4-(2-cyclohexyl-acetylamino)-phenyl ester | HCID 57473678 | — |
Reaction Steps
The title compound was prepared from 4-(2-cyclohexyl-acetylamino)-phenyl chloroformate and 1-cyclopropylmethyl-piperazine, preparative HPLC (method C (60%, off-white crystals). HPLC-MS m/z=400.3 (M+1), Rt: 2.42 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07279470B2 |
| Source dataset | uspto-grants-2007_10 |
| ORD ID | ord-a165884d7f4340edb6332f83e5e0fd0e |
| Source note | uspto-grants-2007_10 |