Carbamic chloride, N-methyl-N-phenyl- → HCID 69519096, compound

HRID 1179976Notes

Reaction equation

HRID 1179976 reaction equation
[OH:1][C:2]1[CH:7]=[CH:6][C:5]([S:8]([NH:11][CH2:12][CH2:13][CH:14]([CH3:16])[CH3:15])(=[O:10])=[O:9])=[CH:4][CH:3]=1.[CH3:17][N:18]([C:22]1[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=1)[C:19](Cl)=[O:20]>>[CH3:15][CH:14]([CH3:16])[CH2:13][CH2:12][NH:11][S:8]([C:5]1[CH:6]=[CH:7][C:2]([O:1][C:19](=[O:20])[N:18]([CH3:17])[C:22]2[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=2)=[CH:3][CH:4]=1)(=[O:10])=[O:9]

Participants

3

Reactant 2

HCID 77969Carbamic chloride, N-methyl-N-phenyl-HCID 22047878HCID 22047878, compound

Product 1

HCID 69519096HCID 69519096, compound

Procedure

The title compound was prepared from 4-hydroxy-N-(3-methyl-butyl)-benzenesulfonamide and N-methyl-N-phenyl carbamoylchloride, preparative HPLC (Method C) (11%, light yellow oil). HPLC-MS m/z=377.2 (M+1), Rt: 4.32 min.

Sources & evidence

ORD record
ord-4bea75dfdf9f498cab7f8fc4c8c9f6c0
Source dataset
uspto-grants-2007_10
Patent number
US07279470B2

Reaction notes

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