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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1179989Generated: October 31, 2026

Diisopropylamine → HCID 69517631, compound

https://huagongshe.com/reaction/1179989

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDiisopropylamineHCID 7912—
Reactant4-(5-Trifluoromethylpyridin-2-yloxy)-phenyl chloroformateHCID 22047762—
ReactantHCID 119931495HCID 119931495—
ProductHCID 69517631HCID 69517631—

Reaction Steps

The title compound was prepared from 4-(5-trifluoromethyl-pyridin-2-yloxy)-phenyl chloroformate and 2-piperidin-4-ylmethyl-2,3-dihydro-1H-isoindole, hydrochloride, 5 equivalent of diisopropylamine was added, preparative HPLC (Method C) (63%, colourless crystals). HPLC-MS m/z=498.1 (M+1), Rt: 3.07 min.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07279470B2
Source datasetuspto-grants-2007_10
ORD IDord-1f413826a4434e33b006cc7c53995984
Source noteuspto-grants-2007_10