tert-Octylamine → HCID 69518263, compound

HRID 1180000Notes

Reaction equation

HRID 1180000 reaction equation
[C:1]([NH2:9])([CH2:4][C:5]([CH3:8])([CH3:7])[CH3:6])([CH3:3])[CH3:2].O=C1CCC(=O)N1[O:17][C:18](=O)[C:19]1[CH:24]=[CH:23][C:22]([O:25][C:26](=[O:35])[N:27]([CH3:34])[C:28]2[CH:33]=[CH:32][CH:31]=[CH:30][CH:29]=2)=[CH:21][CH:20]=1>>[CH3:2][C:1]([NH:9][C:18]([C:19]1[CH:24]=[CH:23][C:22]([O:25][C:26](=[O:35])[N:27]([CH3:34])[C:28]2[CH:29]=[CH:30][CH:31]=[CH:32][CH:33]=2)=[CH:21][CH:20]=1)=[O:17])([CH3:3])[CH2:4][C:5]([CH3:8])([CH3:7])[CH3:6]

Participants

3

Reactant 2

HCID 61017tert-OctylamineHCID 865892064-(Methyl-phenyl-carbamoyloxy)-benzoic Acid 2,5-dioxo-pyrrolidin-1-yl Ester

Product 1

HCID 69518263HCID 69518263, compound

Procedure

The title product was prepared from tert-octylamine and 4-(methyl-phenyl-carbamoyloxy)-benzoic acid 2,5-dioxo-pyrrolidin-1-yl ester, preparative HPLC (method C) (26%, white crystals). HPLC-MS m/z=383.5 (M+1), Rt: 4.67 min.

Sources & evidence

ORD record
ord-96c225bc53f840e5807eab1730c54838
Source dataset
uspto-grants-2007_10
Patent number
US07279470B2

Reaction notes

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