1,2-Ethanediamine, N1,N1,N2-trimethyl- → HCID 69519590, compound

HRID 1180001Notes

Reaction equation

HRID 1180001 reaction equation
[CH3:1][N:2]([CH3:7])[CH2:3][CH2:4][NH:5][CH3:6].O=C1CCC(=O)N1O[C:16](=[O:34])[C:17]1[CH:22]=[CH:21][C:20]([O:23][C:24](=[O:33])[N:25]([CH3:32])[C:26]2[CH:31]=[CH:30][CH:29]=[CH:28][CH:27]=2)=[CH:19][CH:18]=1>>[CH3:1][N:2]([CH3:7])[CH2:3][CH2:4][N:5]([CH3:6])[C:16]([C:17]1[CH:18]=[CH:19][C:20]([O:23][C:24](=[O:33])[N:25]([CH3:32])[C:26]2[CH:27]=[CH:28][CH:29]=[CH:30][CH:31]=2)=[CH:21][CH:22]=1)=[O:34]

Participants

3

Reactant 2

HCID 673381,2-Ethanediamine, N1,N1,N2-trimethyl-HCID 865892064-(Methyl-phenyl-carbamoyloxy)-benzoic Acid 2,5-dioxo-pyrrolidin-1-yl Ester

Product 1

HCID 69519590HCID 69519590, compound

Procedure

The title product was prepared from N,N,N′-trimethylethylendiamine and 4-(methyl-phenyl-carbamoyloxy)-benzoic acid 2,5-dioxo-pyrrolidin-1-yl ester, preparative HPLC (method C) (2%, colourless oil). HPLC-MS m/z=356.2 (M+1), Rt: 2.17 min.

Sources & evidence

ORD record
ord-3808b9caefe74061a9462f80403640bc
Source dataset
uspto-grants-2007_10
Patent number
US07279470B2

Reaction notes

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