Cyclopropanemethanamine → HCID 69518289, compound

HRID 1180002Notes

Reaction equation

HRID 1180002 reaction equation
[CH:1]1([CH2:4][NH2:5])[CH2:3][CH2:2]1.O=C1CCC(=O)N1[O:13][C:14](=O)[C:15]1[CH:20]=[CH:19][C:18]([O:21][C:22](=[O:31])[N:23]([CH3:30])[C:24]2[CH:29]=[CH:28][CH:27]=[CH:26][CH:25]=2)=[CH:17][CH:16]=1>>[CH:1]1([CH2:4][NH:5][C:14]([C:15]2[CH:20]=[CH:19][C:18]([O:21][C:22](=[O:31])[N:23]([CH3:30])[C:24]3[CH:25]=[CH:26][CH:27]=[CH:28][CH:29]=3)=[CH:17][CH:16]=2)=[O:13])[CH2:3][CH2:2]1

Participants

3

Reactant 2

HCID 75646CyclopropanemethanamineHCID 865892064-(Methyl-phenyl-carbamoyloxy)-benzoic Acid 2,5-dioxo-pyrrolidin-1-yl Ester

Product 1

HCID 69518289HCID 69518289, compound

Procedure

The title product was prepared from cyclopropylmethylamine and 4-(methyl-phenyl-carbamoyloxy)-benzoic acid 2,5-dioxo-pyrrolidin-1-yl ester. The crude product was used without further purification (100%, semi-crystal oil). HPLC-MS m/z=325.1 (M+1), Rt: 3.40 min.

Workup

  1. customThe crude product was used without further purification (100%, semi-crystal oil)

Sources & evidence

ORD record
ord-624b5ac4cd80414ea163aaf683d050d5
Source dataset
uspto-grants-2007_10
Patent number
US07279470B2

Reaction notes

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