HuagongsheHuagongshe Chemistry Print Report · For research reference only
1H-Benzimidazole-2-methanamine → HCID 69518755, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1H-Benzimidazole-2-methanamine | HCID 145820 | — |
| Reactant | 4-(Methyl-phenyl-carbamoyloxy)-benzoic Acid 2,5-dioxo-pyrrolidin-1-yl Ester | HCID 86589206 | — |
| Product | HCID 69518755 | HCID 69518755 | — |
Reaction Steps
The title product was prepared from C-(1H-benzimidazol-2-yl)-methylamine and 4-(methyl-phenyl-carbamoyloxy)-benzoic acid 2,5-dioxo-pyrrolidin-1-yl ester. The crude product was subjected to preparative HPLC (method C) (8%, off-white crystals). HPLC-MS m/z=401.1 (M+1), Rt: 2.56 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07279470B2 |
| Source dataset | uspto-grants-2007_10 |
| ORD ID | ord-d7cd9386ab6949c5b23768d3d0e09336 |
| Source note | uspto-grants-2007_10 |