Carbamic chloride, N-methyl-N-phenyl- → HCID 10172002, compound

HRID 1180036Notes

Reaction equation

HRID 1180036 reaction equation
[OH:1][N:2]1[C:6]([S:7][C:8]2[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=2)=[CH:5][CH:4]=[N:3]1.[CH3:14][N:15]([C:19]1[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=1)[C:16](Cl)=[O:17]>>[C:8]1([S:7][C:6]2[N:2]([O:1][C:16](=[O:17])[N:15]([CH3:14])[C:19]3[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=3)[N:3]=[CH:4][CH:5]=2)[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1

Participants

3

Reactant 2

HCID 77969Carbamic chloride, N-methyl-N-phenyl-HCID 22047926HCID 22047926, compound

Product 1

HCID 10172002HCID 10172002, compound

Procedure

The title compound was prepared from 1-hydroxy-5-phenylsulfanylpyrazole and N-methyl-N-phenylcarbamoyl chloride. The crude product was purified by flash chromatography (Quad flash 12, EtOAc-heptane) (80%, oil).

Workup

  1. customThe crude product was purified by flash chromatography (Quad flash 12, EtOAc-heptane) (80%, oil)

Sources & evidence

ORD record
ord-fedde8c6559349d2886ee1ad2d89b179
Source dataset
uspto-grants-2007_10
Patent number
US07279470B2

Reaction notes

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