1-hydroxy-1H-pyrazole → HCID 69519932, compound

HRID 1180056Notes

Reaction equation

HRID 1180056 reaction equation
[OH:1][CH2:2][CH2:3][C:4]1[CH:9]=[CH:8][C:7]([O:10][C:11](=[O:20])[N:12]([CH3:19])[C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=2)=[CH:6][CH:5]=1.O[N:22]1[CH:26]=[CH:25][CH:24]=[N:23]1>>[N:22]1([O:1][CH2:2][CH2:3][C:4]2[CH:5]=[CH:6][C:7]([O:10][C:11](=[O:20])[N:12]([CH3:19])[C:13]3[CH:14]=[CH:15][CH:16]=[CH:17][CH:18]=3)=[CH:8][CH:9]=2)[CH:26]=[CH:25][CH:24]=[N:23]1

Participants

3

Reactant 2

HCID 30167331-hydroxy-1H-pyrazoleHCID 69520342Methyl-phenyl-carbamic Acid 4-(2-hydroxy-ethyl)-phenyl Ester

Product 1

HCID 69519932HCID 69519932, compoundYield 62%

Procedure

The title compound was prepared in 62% yield as an oil using methyl-phenyl-carbamic acid 4-(2-hydroxy-ethyl)-phenyl ester and 1-hydroxypyrazole.

Sources & evidence

ORD record
ord-1afac942c81c49a781f7a729cd1cf5df
Source dataset
uspto-grants-2007_10
Patent number
US07279470B2

Reaction notes

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